Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I03 |
| Synchrotron site | Diamond |
| Beamline | I03 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2016-10-11 |
| Detector | DECTRIS EIGER2 XE 16M |
| Wavelength(s) | 0.97625 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 45.379, 213.655, 55.657 |
| Unit cell angles | 90.00, 96.40, 90.00 |
Refinement procedure
| Resolution | 49.120 - 1.830 |
| R-factor | 0.1811 |
| Rwork | 0.179 |
| R-free | 0.21190 |
| Structure solution method | FOURIER SYNTHESIS |
| RMSD bond length | 0.013 |
| RMSD bond angle | 1.120 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 53.540 | 1.920 |
| High resolution limit [Å] | 1.830 | 1.830 |
| Rmeas | 0.029 | 0.409 |
| Number of reflections | 90887 | 12015 |
| <I/σ(I)> | 17.6 | 2.2 |
| Completeness [%] | 97.9 | 88.9 |
| Redundancy | 3.2 | 2.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 8 | 293 | 0.5M K formate 15% PEG 3350 0.1M pH=8 Bis-Tris propane/HCl |
