Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID29 |
| Synchrotron site | ESRF |
| Beamline | ID29 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2015-09-10 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | .97623 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 46.063, 212.634, 55.987 |
| Unit cell angles | 90.00, 97.16, 90.00 |
Refinement procedure
| Resolution | 49.280 - 2.020 |
| R-factor | 0.21842 |
| Rwork | 0.216 |
| R-free | 0.27183 |
| Structure solution method | FOURIER SYNTHESIS |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.265 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 49.240 | 2.070 |
| High resolution limit [Å] | 2.020 | 2.020 |
| Rmeas | 0.079 | 0.780 |
| Number of reflections | 68408 | 4576 |
| <I/σ(I)> | 8 | |
| Completeness [%] | 98.4 | |
| Redundancy | 3.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 8 | 293 | 0.5M K formate 15% PEG 3350 0.1M pH=8 Bis-Tris propane/HCl |
