8RG1
Soluble glucose dehydrogenase from acinetobacter calcoaceticus - wild type pH8
This is a non-PDB format compatible entry.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE BM07 |
Synchrotron site | ESRF |
Beamline | BM07 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2023-02-06 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.98 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 60.354, 92.508, 84.711 |
Unit cell angles | 90.00, 105.00, 90.00 |
Refinement procedure
Resolution | 42.560 - 1.190 |
R-factor | 0.1484 |
Rwork | 0.148 |
R-free | 0.17280 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.011 |
RMSD bond angle | 1.083 |
Data reduction software | autoPROC |
Data scaling software | autoPROC |
Phasing software | PHASER |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.233 |
High resolution limit [Å] | 1.180 | 1.190 |
Rmerge | 0.420 | |
Rmeas | 0.590 | |
Rpim | 0.420 | |
Number of reflections | 199471 | 1815 |
<I/σ(I)> | 16.5 | |
Completeness [%] | 98.7 | 6.35 |
Redundancy | 6.7 | 2 |
CC(1/2) | 0.999 | 0.648 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 293 | PEG 6000, 100 mM TRIS pH8, 2 mM ZnCl2 |