8QUL
Hexameric HIV-1 CA in complex with DDD00100555
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-07-16 |
Detector | DECTRIS EIGER2 XE 16M |
Wavelength(s) | 0.976 |
Spacegroup name | P 6 |
Unit cell lengths | 90.650, 90.650, 56.680 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 56.680 - 1.670 |
R-factor | 0.177 |
Rwork | 0.175 |
R-free | 0.21000 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.027 |
RMSD bond angle | 2.278 |
Data reduction software | XDS |
Data scaling software | xia2 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 56.680 | 1.700 |
High resolution limit [Å] | 1.670 | 1.670 |
Rmerge | 0.070 | 1.400 |
Number of reflections | 30894 | 1526 |
<I/σ(I)> | 19.4 | 1.8 |
Completeness [%] | 100.0 | 100 |
Redundancy | 10 | 9.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 290 | 0.1M Tris buffer, pH 8.0 to 9.0, 10-15% PEG550MME, 0.15M KSCN |