8QTY
LytR LCP domain from Streptococcus dysgalactiae subs. dysgalactiae
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE MASSIF-1 |
Synchrotron site | ESRF |
Beamline | MASSIF-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-07-21 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.966 |
Spacegroup name | I 4 2 2 |
Unit cell lengths | 141.271, 141.271, 133.742 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.608 - 2.800 |
Rwork | 0.271 |
R-free | 0.29270 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.017 |
RMSD bond angle | 1.968 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | MrBUMP |
Refinement software | REFMAC (5.8.0419) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.608 | 2.950 |
High resolution limit [Å] | 2.800 | 2.800 |
Number of reflections | 16955 | 2436 |
<I/σ(I)> | 15.5 | |
Completeness [%] | 99.9 | |
Redundancy | 8 | |
CC(1/2) | 0.999 | 0.666 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 292 | 2.2 M ammonium sulphate 20% glycerol |