8QPH

Crystal structure of Lymantria dispar CPV14 polyhedra 14 crystals

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE VMXm
Synchrotron site	Diamond
Beamline	VMXm
Temperature [K]	100
Detector technology	PIXEL
Collection date	2021-09-29
Detector	DECTRIS EIGER2 X CdTe 9M
Wavelength(s)	0.5814
Spacegroup name	I 2 3
Unit cell lengths	103.189, 103.189, 103.189
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	72.970 - 1.340
R-factor	0.1571
Rwork	0.156
R-free	0.18030
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.008
RMSD bond angle	1.141
Data reduction software	DIALS
Data scaling software	xia2.multiplex
Phasing software	PHASER
Refinement software	PHENIX (1.20.1_4487)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	72.970	1.388
High resolution limit [Å]	1.340	1.340
Number of reflections	39736	4090
<I/σ(I)>	9.4
Completeness [%]	96.6	98.6
Redundancy	43.3	15.6
CC(1/2)	0.867	0.302

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	IN CELL	7.5	300	In vivo