8Q1J
LSD1 Y391K-CoREST bound to Acetylated K14 of Histone H3
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE MASSIF-1 |
Synchrotron site | ESRF |
Beamline | MASSIF-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-10-08 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.965459 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 118.598, 180.153, 232.678 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.870 - 2.870 |
R-factor | 0.2409 |
Rwork | 0.240 |
R-free | 0.27220 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.285 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.19.2_4158)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.870 | 2.920 |
High resolution limit [Å] | 2.840 | 2.840 |
Rmerge | 0.168 | 3.855 |
Rmeas | 0.188 | 4.429 |
Rpim | 0.082 | 2.114 |
Total number of observations | 279000 | 13875 |
Number of reflections | 57339 | 3421 |
<I/σ(I)> | 6.7 | 0.4 |
Completeness [%] | 97.4 | |
Redundancy | 4.9 | 4.1 |
CC(1/2) | 0.988 | 0.081 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293 | Sodium Tartate 1.2 M, ADA 0.1M |