8PU4
FaRel2 bound to the ATP analogue, APCPP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 2 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 2 |
Temperature [K] | 90 |
Detector technology | PIXEL |
Collection date | 2021-07-28 |
Detector | DECTRIS EIGER X 9M |
Wavelength(s) | 1.0000 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 31.498, 60.581, 177.157 |
Unit cell angles | 90.00, 90.59, 90.00 |
Refinement procedure
Resolution | 59.050 - 2.620 |
R-factor | 0.1972 |
Rwork | 0.194 |
R-free | 0.25540 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.170 |
Refinement software | BUSTER (1.19.2_4158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 59.100 | 2.830 |
High resolution limit [Å] | 2.620 | 2.620 |
Number of reflections | 16326 | 818 |
<I/σ(I)> | 7.3 | |
Completeness [%] | 90.9 | |
Redundancy | 13.5 | |
CC(1/2) | 0.985 | 0.332 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 12 % w/v PEG 2000, 50 mM MES pH 5.5 |