8PPS
Dimeric RbdA EAL, in apo state
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-09-15 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9789 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 64.400, 65.720, 172.250 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.040 - 2.300 |
Rwork | 0.184 |
R-free | 0.23240 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.551 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | MOLREP (11.7.03) |
Refinement software | REFMAC (5.8.0415) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.040 | 2.360 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmeas | 0.059 | 0.918 |
Number of reflections | 31120 | 1890 |
<I/σ(I)> | 15.9 | 1.32 |
Completeness [%] | 93.5 | 78 |
Redundancy | 4.6 | 3.1 |
CC(1/2) | 0.999 | 0.665 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 9 | 294.15 | 100mM Tris and BICINE pH 9 34% (w/v) ethylene glycol and PEG 8000 mix |