8PMY
HEV gt3 P domain in complex with glycan-insensitive nAb p60.15
This is a non-PDB format compatible entry.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PETRA III, DESY BEAMLINE P11 |
Synchrotron site | PETRA III, DESY |
Beamline | P11 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-06-01 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.99987 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 56.190, 122.950, 158.670 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.650 - 2.406 |
R-factor | 0.2135 |
Rwork | 0.212 |
R-free | 0.25040 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 0.960 |
Data reduction software | XDS |
Data scaling software | pointless |
Phasing software | PHASER |
Refinement software | BUSTER (2.10.4) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.640 | 2.492 |
High resolution limit [Å] | 2.406 | 2.406 |
Rmeas | 0.293 | |
Number of reflections | 21742 | 2122 |
<I/σ(I)> | 7.43 | |
Completeness [%] | 99.6 | |
Redundancy | 13.12 | |
CC(1/2) | 0.993 | 0.482 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.5 | 293 | 11% w/v PEG 8000, 0.1M Zinc acetate and 0.1M MES pH 5.5 |