Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I04-1 |
| Synchrotron site | Diamond |
| Beamline | I04-1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2018-07-14 |
| Detector | DECTRIS EIGER X 9M |
| Wavelength(s) | 0.91587 |
| Spacegroup name | I 2 2 2 |
| Unit cell lengths | 63.653, 74.086, 78.739 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 29.660 - 1.440 |
| R-factor | 0.1318 |
| Rwork | 0.130 |
| R-free | 0.15590 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.011 |
| Data reduction software | xia2 |
| Data scaling software | Aimless |
| Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 29.660 | 1.491 |
| High resolution limit [Å] | 1.440 | 1.440 |
| Rmerge | 0.086 | 0.084 |
| Number of reflections | 34084 | 3339 |
| <I/σ(I)> | 20.2 | 3 |
| Completeness [%] | 100.0 | 98.4 |
| Redundancy | 13.2 | 12.7 |
| CC(1/2) | 1.000 | 0.900 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.2 M MAGNESIUM FORMATE, 20 % W/V |
