8PHN
Receiver domain from hybrid Histidine Kinase 3 from Chaetomium thermophilum
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALBA BEAMLINE XALOC |
Synchrotron site | ALBA |
Beamline | XALOC |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-07-22 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97895 |
Spacegroup name | F 4 3 2 |
Unit cell lengths | 154.268, 154.268, 154.268 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 89.070 - 1.900 |
R-factor | 0.21169 |
Rwork | 0.211 |
R-free | 0.22200 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.005 |
RMSD bond angle | 1.145 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0403) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 89.070 | 1.940 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.088 | 1.245 |
Rmeas | 0.090 | 1.275 |
Rpim | 0.020 | 0.272 |
Total number of observations | 275556 | 17418 |
Number of reflections | 12954 | 803 |
<I/σ(I)> | 22.3 | 3 |
Completeness [%] | 100.0 | |
Redundancy | 21.3 | 21.7 |
CC(1/2) | 1.000 | 0.836 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 294 | 2M ammonium sulphate 0.1 M Tris pH 8.5 |