8PC4
MEMBRANE TARGET COMPLEX 1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ELETTRA BEAMLINE 11.2C |
Synchrotron site | ELETTRA |
Beamline | 11.2C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-07-31 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.0000 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 94.389, 94.389, 442.325 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 54.750 - 2.850 |
R-factor | 0.2669 |
Rwork | 0.265 |
R-free | 0.30110 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.261 |
Data reduction software | MOSFLM |
Data scaling software | Aimless |
Phasing software | PHENIX |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 88.470 | 3.020 |
High resolution limit [Å] | 2.660 | 2.860 |
Rmerge | 0.142 | 1.500 |
Number of reflections | 35073 | 4539 |
<I/σ(I)> | 8.7 | |
Completeness [%] | 100.0 | |
Redundancy | 11.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 293 | Lithium Sulfate |