8P96

TARGET COMPLEX 3

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ELETTRA BEAMLINE 11.2C
Synchrotron site	ELETTRA
Beamline	11.2C
Temperature [K]	100
Detector technology	PIXEL
Collection date	2019-07-31
Detector	DECTRIS PILATUS 2M
Wavelength(s)	1.000
Spacegroup name	P 65 2 2
Unit cell lengths	94.349, 94.349, 444.751
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	65.840 - 2.860
R-factor	0.2539
Rwork	0.253
R-free	0.28080
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.005
RMSD bond angle	1.018
Data reduction software	iMOSFLM
Data scaling software	Aimless
Refinement software	PHENIX (1.20.1_4487)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	81.710	3.010
High resolution limit [Å]	2.860	2.860
Number of reflections	28271	3913
<I/σ(I)>	4.7
Completeness [%]	99.4
Redundancy	11.9
CC(1/2)	0.300	0.300

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION		293	1M LITHIUM SULFATE