8OW6
PERIDININ-CHLOROPHYLL-PROTEIN OF HETEROCAPSA PYGMAEA, 100K
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-11-15 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 0.9788 |
Spacegroup name | P 3 1 2 |
Unit cell lengths | 90.610, 90.610, 155.610 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 43.500 - 1.200 |
R-factor | 0.1626 |
Rwork | 0.149 |
R-free | 0.17050 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.014 |
RMSD bond angle | 1.027 |
Data reduction software | XDS (VERSION Feb 5, 2021 BUILT=20210323) |
Data scaling software | XSCALE (VERSION Feb 5, 2021 BUILT=20210323) |
Phasing software | PHASER |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 43.500 | 1.230 |
High resolution limit [Å] | 1.200 | 1.200 |
Rmerge | 0.107 | 0.782 |
Rmeas | 0.119 | 0.942 |
Number of reflections | 227100 | 16634 |
<I/σ(I)> | 8.11 | 1.31 |
Completeness [%] | 99.9 | |
Redundancy | 5.2 | |
CC(1/2) | 0.995 | 0.386 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 291.15 | 0.82 M NaH2PO4 1.24 M K2HPO4 100 mM Na-acetate at pH 5.5 100 mM LiSO4 |