8OVQ
Crystal structure of Geodia cydonium sponge adhesion molecule long form (SAML).
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALBA BEAMLINE XALOC |
Synchrotron site | ALBA |
Beamline | XALOC |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-11-18 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97926 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 33.080, 41.160, 77.801 |
Unit cell angles | 90.00, 90.01, 90.00 |
Refinement procedure
Resolution | 38.931 - 1.610 |
Rwork | 0.151 |
R-free | 0.20270 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.554 |
Data reduction software | XDS (BUILT=20220110) |
Data scaling software | XDS (0.7.9) |
Phasing software | PHASER (2.8.3) |
Refinement software | REFMAC (5.8.0415) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 77.800 | 1.640 |
High resolution limit [Å] | 1.610 | 1.610 |
Rmerge | 0.067 | 0.740 |
Rmeas | 0.088 | |
Rpim | 0.056 | |
Number of reflections | 27255 | 1358 |
<I/σ(I)> | 9.3 | 1.5 |
Completeness [%] | 99.5 | 99.6 |
Redundancy | 4.1 | 3.7 |
CC(1/2) | 0.997 | 0.576 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 295 | PEG4000, 0.2M ammonium sulfate |