8OV9
Crystal structure of Ene-reductase 1 from black poplar mushroom
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PETRA III, EMBL c/o DESY BEAMLINE P13 (MX1) |
Synchrotron site | PETRA III, EMBL c/o DESY |
Beamline | P13 (MX1) |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-11-12 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.9763 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 58.310, 59.308, 208.365 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 41.580 - 1.410 |
R-factor | 0.1259 |
Rwork | 0.124 |
R-free | 0.15270 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.051 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (dev_4788) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 41.580 | 1.430 |
High resolution limit [Å] | 1.410 | 1.410 |
Rmerge | 0.068 | 0.444 |
Rmeas | 0.070 | 0.501 |
Rpim | 0.019 | 0.229 |
Number of reflections | 867680 | 6759 |
<I/σ(I)> | 21.57 | 2.99 |
Completeness [%] | 97.3 | 50.76 |
Redundancy | 12.8 | 4.6 |
CC(1/2) | 0.999 | 0.856 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 9 | 293 | 0.1 M Bicine pH 9.0, 1.6 M Ammonium sulfate 9 |