Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I04-1 |
| Synchrotron site | Diamond |
| Beamline | I04-1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2016-02-03 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.97949 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 30.863, 69.346, 62.473 |
| Unit cell angles | 90.00, 96.85, 90.00 |
Refinement procedure
| Resolution | 46.230 - 1.600 |
| Rwork | 0.190 |
| R-free | 0.23460 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.013 |
| RMSD bond angle | 1.848 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | BALBES |
| Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 46.230 | 1.630 |
| High resolution limit [Å] | 1.600 | 1.600 |
| Rmerge | 0.116 | 0.933 |
| Rmeas | 0.120 | 0.968 |
| Rpim | 0.032 | 0.258 |
| Number of reflections | 34197 | 1687 |
| <I/σ(I)> | 11 | 2.7 |
| Completeness [%] | 99.1 | 97.1 |
| Redundancy | 13.8 | 13.9 |
| CC(1/2) | 0.995 | 0.967 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 5 | 293 | 2 M sodium formate, 0.1 M sodium acetate, pH 5.0 |
