8OUN
Arf GTPase from the asgard Gerdarchaea : GerdArfR1 bound to GDP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 2 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-09-24 |
Detector | DECTRIS EIGER X 9M |
Wavelength(s) | 0.980097 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 43.290, 59.930, 72.350 |
Unit cell angles | 90.00, 102.09, 90.00 |
Refinement procedure
Resolution | 45.730 - 1.653 |
R-factor | 0.2136 |
Rwork | 0.212 |
R-free | 0.24020 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 0.970 |
Data reduction software | autoPROC |
Data scaling software | autoPROC |
Phasing software | PHASER |
Refinement software | BUSTER (2.10.4 (20-OCT-2021)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.730 | 1.710 |
High resolution limit [Å] | 1.650 | 1.650 |
Rmeas | 0.070 | 0.730 |
Number of reflections | 39833 | 2142 |
<I/σ(I)> | 14.8 | |
Completeness [%] | 91.8 | |
Redundancy | 5.4 | |
CC(1/2) | 0.999 | 0.734 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 290 | 18% PEG 8000, 0.2 M Calcium acetate, 0.1M Sodium cacodylate pH 6.5 |