8OUL
Arf GTPase from the asgard Hodarchaea : HodArfR1 bound to GDP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-08-16 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.97856 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 75.693, 75.693, 189.306 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.470 - 3.100 |
R-factor | 0.239 |
Rwork | 0.236 |
R-free | 0.28930 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.000 |
Data reduction software | XDS |
Data scaling software | STARANISO |
Phasing software | PHASER |
Refinement software | BUSTER (2.10.4 (20-OCT-2021)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 70.300 | 3.290 |
High resolution limit [Å] | 3.100 | 3.100 |
Rmeas | 0.048 | 0.269 |
Number of reflections | 10627 | 1678 |
<I/σ(I)> | 6.2 | 1.1 |
Completeness [%] | 99.9 | 99.9 |
Redundancy | 18.3 | |
CC(1/2) | 0.994 | 0.063 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 290 | 30% PEG 4000, 0.1M Tris-HCl pH 8.5, 0.2M Lithium sulfate |