Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID23-1 |
| Synchrotron site | ESRF |
| Beamline | ID23-1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2019-07-25 |
| Detector | DECTRIS PILATUS3 6M |
| Wavelength(s) | 0.9763 |
| Spacegroup name | P 1 |
| Unit cell lengths | 92.161, 92.365, 92.391 |
| Unit cell angles | 120.12, 98.91, 108.97 |
Refinement procedure
| Resolution | 46.121 - 1.370 |
| Rwork | 0.187 |
| R-free | 0.20610 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 80.310 | 2.030 |
| High resolution limit [Å] | 1.370 | 1.370 |
| Number of reflections | 482862 | 284282 |
| <I/σ(I)> | 8.69 | |
| Completeness [%] | 90.4 | |
| Redundancy | 1.2 | |
| CC(1/2) | 0.970 | 0.870 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 7.3 | 290 | TRIS-HCl |
