8OMS

X-ray structure of lysozyme obtained upon reaction with [VIVO(empp)2] (Structure B)

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ELETTRA BEAMLINE 11.2C
Synchrotron site	ELETTRA
Beamline	11.2C
Temperature [K]	100
Detector technology	PIXEL
Collection date	2021-11-10
Detector	DECTRIS PILATUS 6M
Wavelength(s)	1.00
Spacegroup name	P 43 21 2
Unit cell lengths	77.590, 77.590, 37.580
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	38.803 - 1.100
Rwork	0.144
R-free	0.16700
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.021
RMSD bond angle	2.691
Data reduction software	autoPROC
Data scaling software	autoPROC
Phasing software	PHASER
Refinement software	REFMAC (5.8.0267)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	55.260	1.220
High resolution limit [Å]	1.080	1.080
Number of reflections	46747	2164
<I/σ(I)>	28.8
Completeness [%]	99.4
Redundancy	17.6
CC(1/2)	0.999	0.867

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	7	293	0.8 M succinic acid at pH 7.0