8OM8

X-ray structure of lysozyme obtained upon reaction with [VIVO(empp)2] (Structure A)

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ELETTRA BEAMLINE 11.2C
Synchrotron site	ELETTRA
Beamline	11.2C
Temperature [K]	100
Detector technology	PIXEL
Collection date	2022-07-28
Detector	DECTRIS PILATUS 6M
Wavelength(s)	1.0
Spacegroup name	P 43 21 2
Unit cell lengths	78.060, 78.060, 37.010
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	55.258 - 1.080
Rwork	0.148
R-free	0.18950
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.022
RMSD bond angle	2.967
Data reduction software	autoPROC
Data scaling software	autoPROC
Phasing software	PHASER
Refinement software	REFMAC (5.8.0267)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	55.400	1.100
High resolution limit [Å]	1.080	1.080
Number of reflections	50384	2483
<I/σ(I)>	33.2
Completeness [%]	100.0
Redundancy	20
CC(1/2)	1.000	0.744

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	4	293	1.1 M sodium chloride, 0.1 M sodium acetate pH 4.0