8KGA
SlNDPS1-AtcPT4 Chimera
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL32XU |
Synchrotron site | SPring-8 |
Beamline | BL32XU |
Temperature [K] | 80 |
Detector technology | PIXEL |
Collection date | 2022-12-17 |
Detector | DECTRIS EIGER X 9M |
Wavelength(s) | 1.0 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 58.110, 90.107, 126.479 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.883 - 2.182 |
Rwork | 0.203 |
R-free | 0.25000 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.005 |
RMSD bond angle | 1.275 |
Data reduction software | DIALS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0411) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.310 |
High resolution limit [Å] | 2.180 | 2.180 |
Rmeas | 0.131 | 3.060 |
Number of reflections | 465239 | 10711 |
<I/σ(I)> | 9.74 | 0.72 |
Completeness [%] | 99.9 | 99.5 |
Redundancy | 7 | 7 |
CC(1/2) | 0.998 | 0.576 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 293 | Sodium malonate, PEG 3350 |