8KFS
Crystal structure of ZmMOC1/nicked Holliday junction complex at ground state
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-05-01 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.978 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 54.263, 78.028, 63.456 |
Unit cell angles | 90.00, 98.11, 90.00 |
Refinement procedure
Resolution | 19.510 - 2.150 |
R-factor | 0.2043 |
Rwork | 0.203 |
R-free | 0.22750 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6jrg |
RMSD bond length | 0.008 |
RMSD bond angle | 0.882 |
Data reduction software | autoPROC |
Data scaling software | autoPROC |
Phasing software | PHASER |
Refinement software | PHENIX (1.21rc1_4958) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.310 |
High resolution limit [Å] | 2.150 | 2.150 |
Rmerge | 0.143 | 0.763 |
Number of reflections | 28620 | 5689 |
<I/σ(I)> | 13.02 | 2.5 |
Completeness [%] | 97.9 | 99.7 |
Redundancy | 6.8 | |
CC(1/2) | 0.837 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | 6% Isopropyl alcohol, 0.1 M Sodium acetate pH5.0, 35% Polyethylene glycol monomethyl ether 550 |