8KDL
Crystal structure of LmbF in complex with PLP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-1A |
Synchrotron site | Photon Factory |
Beamline | BL-1A |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-11-14 |
Detector | DECTRIS EIGER X 4M |
Wavelength(s) | 1.1 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 67.277, 74.017, 74.843 |
Unit cell angles | 90.00, 93.18, 90.00 |
Refinement procedure
Resolution | 48.630 - 1.700 |
R-factor | 0.1658 |
Rwork | 0.165 |
R-free | 0.20400 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 0.979 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.630 | 1.730 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.113 | 0.488 |
Number of reflections | 80638 | 4199 |
<I/σ(I)> | 11.8 | 3 |
Completeness [%] | 99.9 | 98.7 |
Redundancy | 7 | |
CC(1/2) | 0.997 | 0.841 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.1M MES pH 6.5, 27% PEG 4000, 0.8M LiCl |