8KCV
Crystal structure of UDA01-CAAMDDFQL
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2023-04-30 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 1.0 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 91.446, 108.524, 125.310 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.970 - 2.390 |
R-factor | 0.2088 |
Rwork | 0.207 |
R-free | 0.25060 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.040 |
Data reduction software | autoPROC |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.20.1_4487: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 108.520 | 2.510 |
High resolution limit [Å] | 2.390 | 2.390 |
Rmerge | 0.135 | 0.692 |
Rmeas | 0.151 | 0.769 |
Rpim | 0.065 | 0.327 |
Total number of observations | 204163 | 31003 |
Number of reflections | 41604 | 6216 |
<I/σ(I)> | 9.3 | 2.4 |
Completeness [%] | 83.1 | |
Redundancy | 4.9 | 5 |
CC(1/2) | 0.994 | 0.808 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | LIQUID DIFFUSION | 277.15 | BIS-TRIS pH7.5 PEG3350 |