8KB0
Crystal structure of 01JD-AEAIIVAMV
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2023-06-09 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 1.0 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 85.706, 89.237, 117.850 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.990 - 2.480 |
R-factor | 0.208 |
Rwork | 0.203 |
R-free | 0.27540 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.031 |
Data reduction software | autoPROC |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.20.1_4487: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 71.140 | 2.610 |
High resolution limit [Å] | 2.480 | 2.480 |
Rmerge | 0.132 | 1.159 |
Rmeas | 0.138 | 1.204 |
Rpim | 0.038 | 0.324 |
Total number of observations | 398097 | 64311 |
Number of reflections | 30537 | 4712 |
<I/σ(I)> | 14.6 | 2.5 |
Completeness [%] | 92.7 | |
Redundancy | 13 | 13.6 |
CC(1/2) | 0.999 | 0.888 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | LIPIDIC CUBIC PHASE | 277.15 | 0.2M Ammonium acetate 0.1M HEPES pH 7.5 25% w/v PEG 3350 |