8K48
LTD of arabidopsis thaliana
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-09-08 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.9790 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 63.776, 63.776, 225.397 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 28.860 - 2.100 |
Rwork | 0.228 |
R-free | 0.24490 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.008 |
Data reduction software | HKL-2000 |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.17.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 28.860 | 2.175 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.087 | 0.506 |
Number of reflections | 28181 | 2716 |
<I/σ(I)> | 29.68 | 5.43 |
Completeness [%] | 99.9 | |
Redundancy | 6.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 289 | 0.1M Sodium acetate, 0.2M Calcium chloride, 10% isopropanol |