8K1W
Crystal structure of PLA2 from Saccharothrix espanaensis
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-01-14 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.9796 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 32.741, 37.679, 84.557 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 34.417 - 1.302 |
R-factor | 0.152838555594 |
Rwork | 0.153 |
R-free | 0.15688 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 1.068 |
Data scaling software | HKL-3000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692+SVN) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.320 |
High resolution limit [Å] | 1.300 | 1.300 |
Number of reflections | 26771 | 1276 |
<I/σ(I)> | 25 | |
Completeness [%] | 100.0 | |
Redundancy | 11.9 | |
CC(1/2) | 0.994 | 0.962 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 293 | 0.1 M Tris-HCl, pH 8.5, 30% 2-Propanol, 30% PEG 3350 |