8JXK

Crystal Structure of Rv0047c from Mycobacterium tuberculosis

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU FR-E+ SUPERBRIGHT
Temperature [K]	100
Detector technology	IMAGE PLATE
Collection date	2019-05-08
Detector	RIGAKU RAXIS IV++
Wavelength(s)	1.54178
Spacegroup name	P 61
Unit cell lengths	102.170, 102.170, 191.880
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	30.076 - 3.150
Rwork	0.204
R-free	0.25260
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.007
RMSD bond angle	1.534
Data reduction software	iMOSFLM
Data scaling software	Aimless
Phasing software	PHASER
Refinement software	REFMAC (5.8.0258)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	30.080	3.370
High resolution limit [Å]	3.150	3.150
Number of reflections	17786	3098
<I/σ(I)>	22.1
Completeness [%]	90.7
Redundancy	12.9
CC(1/2)	0.990	0.940

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		295	0.1M Sodium Acetate, 1.8M Sodium Formate