8JPV
Glutamyl-tRNA synthetase from Methylacidiphilum fumariolicum
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU R-AXIS IV |
Temperature [K] | 110 |
Detector technology | IMAGE PLATE |
Collection date | 2017-07-27 |
Detector | RIGAKU RAXIS IV |
Wavelength(s) | 1.5419 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 40.310, 62.540, 190.280 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 95.140 - 2.510 |
R-factor | 0.21174 |
Rwork | 0.209 |
R-free | 0.26574 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.316 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0135) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 95.140 | 7.940 |
High resolution limit [Å] | 2.510 | 2.510 |
Rmerge | 0.161 | |
Number of reflections | 16313 | 17211 |
<I/σ(I)> | 9.5 | |
Completeness [%] | 99.8 | |
Redundancy | 6.2 | |
CC(1/2) | 0.993 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7 | 293 | HEPES buffer pH 7.0, 10% PEG 6000, 200 mM NaSCN |