8JMS
Crystal structure of BelL from Streptomyces cavourensis
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-08-27 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1.0 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 62.618, 62.618, 122.464 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 44.280 - 2.200 |
R-factor | 0.1976 |
Rwork | 0.193 |
R-free | 0.23640 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 0.867 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.280 | 2.270 |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.154 | 0.917 |
Number of reflections | 12865 | 1096 |
<I/σ(I)> | 14.6 | 3.3 |
Completeness [%] | 99.1 | 99 |
Redundancy | 13 | |
CC(1/2) | 0.997 | 0.849 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.1M magnesium diformate, 25% w/v PEG 3350, 0.05M CsCl |