8JH0
Crystal structure of the light-driven sodium pump IaNaR
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL41XU |
Synchrotron site | SPring-8 |
Beamline | BL41XU |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-12-02 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 1.0 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 67.435, 71.770, 123.860 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.140 - 2.790 |
R-factor | 0.2452 |
Rwork | 0.243 |
R-free | 0.28700 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.004 |
RMSD bond angle | 0.686 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHENIX ((1.19.2_4158)) |
Refinement software | PHENIX ((1.19.2_4158)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.960 |
High resolution limit [Å] | 2.790 | 2.790 |
Number of reflections | 15200 | 2189 |
<I/σ(I)> | 13.6 | 2.1 |
Completeness [%] | 98.1 | 89.5 |
Redundancy | 6.3 | 5 |
CC(1/2) | 0.999 | 0.803 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | LIPIDIC CUBIC PHASE | 5.1 | 293 | Ammonium Nitrate, sodium citrate, PEG 350 MME |