8JG7
Serine decarboxylase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-05-16 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.979 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 115.360, 149.450, 139.126 |
Unit cell angles | 90.00, 109.18, 90.00 |
Refinement procedure
Resolution | 49.390 - 2.850 |
R-factor | 0.21591 |
Rwork | 0.214 |
R-free | 0.26180 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.410 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0352) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.900 |
High resolution limit [Å] | 2.850 | 7.730 | 2.850 |
Rmerge | 0.173 | 0.165 | 0.551 |
Rmeas | 0.189 | 0.180 | 0.616 |
Rpim | 0.076 | 0.070 | 0.270 |
Number of reflections | 52125 | 2685 | 2556 |
<I/σ(I)> | 3.5 | ||
Completeness [%] | 99.6 | 100 | 98.1 |
Redundancy | 5.9 | 6.4 | 5 |
CC(1/2) | 0.860 | 0.904 | 0.846 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 289.15 | 20% PEG 400, 0.2M CaCl2, PH8.0 |