Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL10U2 |
Synchrotron site | SSRF |
Beamline | BL10U2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-08-25 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.979021 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 104.388, 104.388, 145.334 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 56.640 - 2.860 |
R-factor | 0.2045 |
Rwork | 0.202 |
R-free | 0.24990 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.005 |
RMSD bond angle | 0.730 |
Data reduction software | autoPROC |
Data scaling software | autoPROC |
Phasing software | PHENIX (1.20.1_4487) |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 90.400 | 3.010 |
High resolution limit [Å] | 2.860 | 2.860 |
Number of reflections | 21144 | 3146 |
<I/σ(I)> | 15.1 | |
Completeness [%] | 96.9 | |
Redundancy | 10.3 | |
CC(1/2) | 0.998 | 0.895 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 291.15 | 31% PEG1500,0.1M Tris pH 8.4 |