8IPG
Structure of HP101/N44
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X10SA |
| Synchrotron site | SLS |
| Beamline | X10SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2022-11-07 |
| Detector | DECTRIS EIGER2 X 16M |
| Wavelength(s) | 1.000 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 71.387, 41.609, 85.309 |
| Unit cell angles | 90.00, 109.69, 90.00 |
Refinement procedure
| Resolution | 40.160 - 1.640 |
| R-factor | 0.2488 |
| Rwork | 0.247 |
| R-free | 0.28800 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.007 |
| RMSD bond angle | 0.944 |
| Data reduction software | XDS |
| Data scaling software | HKL-2000 |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.10.1_2155) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 40.161 | 1.740 |
| High resolution limit [Å] | 1.639 | 1.639 |
| Rmerge | 0.125 | 1.049 |
| Number of reflections | 56809 | 9187 |
| <I/σ(I)> | 5.27 | |
| Completeness [%] | 97.3 | 91.7 |
| Redundancy | 3.347 | 2.835 |
| CC(1/2) | 0.985 | 0.447 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6 | 291 | PEG 3350, 0.2M Ammonium sulfate |
