8INA

Crystal structure of UGT74AN3-UDP

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL19U1
Synchrotron site	SSRF
Beamline	BL19U1
Temperature [K]	291.15
Detector technology	PIXEL
Collection date	2021-03-26
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.97915
Spacegroup name	P 21 21 21
Unit cell lengths	45.741, 52.667, 202.111
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	19.870 - 1.860
R-factor	0.1887
Rwork	0.187
R-free	0.22130
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.009
RMSD bond angle	0.950
Data reduction software	XDS (1.19.2_4158)
Data scaling software	Aimless
Refinement software	PHENIX (1.19.2_4158)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	19.870	1.900
High resolution limit [Å]	1.860	1.860
Number of reflections	42077	2699
<I/σ(I)>	9.6
Completeness [%]	99.9
Redundancy	12.8
CC(1/2)	0.991	0.909

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		291.15	PEG2000MME, 0.1M Hepes (7.5), 0.2M potassium nitro