8IGT
Crystal Structure of Intracellular B30.2 Domain of BTN2A1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-07-22 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9793 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 73.957, 78.889, 41.682 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 28.670 - 1.560 |
R-factor | 0.1558 |
Rwork | 0.155 |
R-free | 0.17320 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5zxk |
RMSD bond length | 0.014 |
RMSD bond angle | 1.824 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0238) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 1.590 |
High resolution limit [Å] | 1.560 | 4.230 | 1.560 |
Rmerge | 0.095 | 0.052 | 0.471 |
Rmeas | 0.099 | 0.054 | 0.495 |
Rpim | 0.027 | 0.015 | 0.151 |
Total number of observations | 454210 | ||
Number of reflections | 35687 | 1955 | 1647 |
<I/σ(I)> | 4.7 | ||
Completeness [%] | 99.6 | 99.4 | 93.5 |
Redundancy | 12.7 | 11.9 | 10.1 |
CC(1/2) | 0.998 | 0.947 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 289 | 0.4 M potassium sodium tartrate |