8I3X

Rice APIP6-RING homodimer

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL19U1
Synchrotron site	SSRF
Beamline	BL19U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2018-01-05
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.979
Spacegroup name	P 21 21 21
Unit cell lengths	34.239, 46.577, 83.182
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	40.640 - 1.780
R-factor	0.1878
Rwork	0.186
R-free	0.23180
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.005
RMSD bond angle	0.743
Data reduction software	XDS
Data scaling software	XDS
Phasing software	PHASER
Refinement software	PHENIX (1.12_2829)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	40.640	1.844
High resolution limit [Å]	1.780	1.780
Number of reflections	13316	1294
<I/σ(I)>	40.5
Completeness [%]	99.9
Redundancy	12.1
CC(1/2)	0.994	0.988

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION		291	ammonium fluoride, PEG 3350