8HP4
CtPDC complex
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SEALED TUBE |
| Source details | BRUKER D8 QUEST |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2022-03-15 |
| Detector | Bruker PHOTON II |
| Wavelength(s) | 1.54178 |
| Spacegroup name | I 1 2 1 |
| Unit cell lengths | 116.420, 87.550, 118.260 |
| Unit cell angles | 90.00, 114.06, 90.00 |
Refinement procedure
| Resolution | 43.780 - 2.520 |
| R-factor | 0.20947 |
| Rwork | 0.207 |
| R-free | 0.25368 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2vjy |
| RMSD bond length | 0.004 |
| RMSD bond angle | 1.301 |
| Data reduction software | Aimless |
| Refinement software | REFMAC |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 43.780 | 2.620 |
| High resolution limit [Å] | 2.520 | 2.520 |
| Rmerge | 0.516 | |
| Number of reflections | 35596 | 3757 |
| <I/σ(I)> | 7.1 | |
| Completeness [%] | 96.7 | |
| Redundancy | 2.5 | |
| CC(1/2) | 0.967 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.2 M sodium malonate pH 5.5, 18% Polyethylene glycol 3350 |
