8HP0
Crystal structure of meso-diaminopimelate dehydrogenase from Prevotella timonensis
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SEALED TUBE |
Source details | BRUKER D8 QUEST |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-02-28 |
Detector | Bruker PHOTON II |
Wavelength(s) | 1.54178 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 101.750, 190.470, 101.150 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 44.910 - 2.470 |
R-factor | 0.22624 |
Rwork | 0.224 |
R-free | 0.26561 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.004 |
RMSD bond angle | 1.271 |
Data scaling software | Aimless |
Refinement software | REFMAC (5) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.870 | 2.570 |
High resolution limit [Å] | 2.470 | 2.470 |
Rmerge | 0.066 | 0.507 |
Number of reflections | 35517 | 3948 |
<I/σ(I)> | 13.3 | |
Completeness [%] | 99.7 | 99.4 |
Redundancy | 4.2 | 3.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 298 | 0.1 M HEPES, pH 7.5, and 0.1 M ammonium sulfate |