8HLG
Crystal structure of MoaE
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 95 |
Detector technology | PIXEL |
Collection date | 2019-10-24 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.9792 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 62.020, 94.950, 101.110 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.650 - 2.000 |
R-factor | 0.1965 |
Rwork | 0.194 |
R-free | 0.23560 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.005 |
RMSD bond angle | 0.722 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | BALBES |
Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 30.000 | 30.000 | 2.050 |
High resolution limit [Å] | 2.000 | 8.940 | 2.000 |
Rmerge | 0.057 | 0.028 | 0.560 |
Rmeas | 0.062 | 0.031 | 0.608 |
Number of reflections | 20539 | 264 | 1477 |
<I/σ(I)> | 16.56 | ||
Completeness [%] | 99.9 | ||
Redundancy | 6.4 | ||
CC(1/2) | 0.999 | 0.999 | 0.909 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 293 | Lithium Sulfate, Tris-HCl, PEG 3350 |