8HEL
Crystal Structure of Anti-CRISPR AcrIE3
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 7A (6B, 6C1) |
Synchrotron site | PAL/PLS |
Beamline | 7A (6B, 6C1) |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2021-05-03 |
Detector | ADSC QUANTUM 270 |
Wavelength(s) | 0.9792 |
Spacegroup name | I 41 2 2 |
Unit cell lengths | 58.353, 58.353, 90.633 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 25.077 - 1.332 |
R-factor | 0.1944 |
Rwork | 0.191 |
R-free | 0.22920 |
Structure solution method | SAD |
RMSD bond length | 0.006 |
RMSD bond angle | 0.835 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX (1.9_1692) |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 1.380 |
High resolution limit [Å] | 1.330 | 2.870 | 1.330 |
Rmerge | 0.963 | 0.067 | 1.889 |
Total number of observations | 502158 | ||
Number of reflections | 18288 | 3412 | 3357 |
<I/σ(I)> | 8.1 | ||
Completeness [%] | 99.9 | 98.8 | 100 |
Redundancy | 14.7 | 14.1 | 13.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 277 | 1.25 M 1,6-hexanediol, 10 mM cobalt(II) chloride hexahydrate, 100 mM sodium acetate, pH 3.7 |