8H8L
Crystal structure of apo-R52F/E56F/R59F/E63F-rHLFr
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU PhotonJet-R |
Temperature [K] | 93 |
Detector technology | PIXEL |
Collection date | 2022-03-01 |
Detector | RIGAKU HyPix-6000HE |
Wavelength(s) | 1.5418 |
Spacegroup name | F 4 3 2 |
Unit cell lengths | 181.310, 181.310, 181.310 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.279 - 1.500 |
Rwork | 0.156 |
R-free | 0.17120 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1dat |
RMSD bond length | 0.014 |
RMSD bond angle | 1.886 |
Data reduction software | CrysalisPro |
Data scaling software | Aimless |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.279 | 1.530 |
High resolution limit [Å] | 1.500 | 1.500 |
Number of reflections | 41282 | 2010 |
<I/σ(I)> | 30.4 | |
Completeness [%] | 100.0 | |
Redundancy | 10.2 | |
CC(1/2) | 1.000 | 0.951 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | Ammonium sulphate, Cadmium sulphate |