8GPB

STRUCTURAL MECHANISM FOR GLYCOGEN PHOSPHORYLASE CONTROL BY PHOSPHORYLATION AND AMP

Experimental procedure

Spacegroup name	P 43 21 2
Unit cell lengths	128.500, 128.500, 116.300
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	? - 2.200
Rwork	0.206
RMSD bond length	0.018
RMSD bond angle	3.600
Refinement software	X-PLOR

Data quality characteristics

	Overall
High resolution limit [Å]	2.200 *
Rmerge	0.080 *
Total number of observations	165007 *
Number of reflections	36295 *
Completeness [%]	80.0 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Batch method *		16 *	took Johnson et al., 1974 from original paper *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	1	dithiothreitol	0.3 (M)
2	1	1	magnesium acetate	1 (M)
3	1	1	IMP	0.2 (M)
4	1	1		0.2 (mM)
5	1	1	sodium azide	0.03 (%)