8GMM

Stenotrophomonas maltophilia Holo HphA

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	CLSI BEAMLINE 08ID-1
Synchrotron site	CLSI
Beamline	08ID-1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2018-06-05
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.9795
Spacegroup name	P 1 21 1
Unit cell lengths	46.618, 76.663, 62.264
Unit cell angles	90.00, 94.33, 90.00

Refinement procedure

Resolution	48.250 - 1.800
R-factor	0.153
Rwork	0.152
R-free	0.17850
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.007
RMSD bond angle	0.906
Data reduction software	HKL-3000
Data scaling software	HKL-3000
Refinement software	PHENIX ((1.20.1_4487: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	48.250	1.864
High resolution limit [Å]	1.800	1.800
Number of reflections	35631	1470
<I/σ(I)>	13.86
Completeness [%]	82.3
Redundancy	5.2
CC(1/2)	0.997	0.829

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293	0.1 M Tris-HCL pH8.5, 25% (w/v) PEG3350