8FQJ
LSD1-CoREST in complex with T14, short soaking
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID30B |
Synchrotron site | ESRF |
Beamline | ID30B |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-06-22 |
Detector | DECTRIS EIGER X 9M |
Wavelength(s) | 0.965459 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 118.883, 179.340, 233.389 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.400 - 2.900 |
R-factor | 0.2188 |
Rwork | 0.218 |
R-free | 0.24560 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.011 |
RMSD bond angle | 1.534 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.18.2) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.560 | 2.980 |
High resolution limit [Å] | 2.900 | 2.900 |
Rmerge | 0.143 | 1.625 |
Rmeas | 0.163 | 1.872 |
Rpim | 0.076 | 0.902 |
Total number of observations | 224031 | 17067 |
Number of reflections | 54215 | 4399 |
<I/σ(I)> | 7.8 | 0.9 |
Completeness [%] | 97.9 | |
Redundancy | 4.1 | 3.9 |
CC(1/2) | 0.993 | 0.280 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293 | 1.2 Na/K Tartrate, 100 mM ADA pH 6.5 |