8F2Z
LSD1-CoREST in complex with AW2, short soaking
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-01-28 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.999869 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 119.474, 179.246, 234.683 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.710 - 3.000 |
R-factor | 0.2156 |
Rwork | 0.214 |
R-free | 0.24630 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2v1d |
RMSD bond length | 0.010 |
RMSD bond angle | 1.394 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.18.2) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.710 | 3.100 |
High resolution limit [Å] | 3.000 | 3.000 |
Rmerge | 0.158 | 3.570 |
Rmeas | 0.171 | 3.847 |
Rpim | 0.065 | 1.426 |
Total number of observations | 345622 | 32912 |
Number of reflections | 50643 | 4598 |
<I/σ(I)> | 8.7 | 0.8 |
Completeness [%] | 99.9 | |
Redundancy | 6.8 | 7.2 |
CC(1/2) | 0.996 | 0.384 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293 | 1.2 M Na/K Tartrate, 100 mM ADA pH 6.5 |