8EV2
Dual Modulators
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-BM |
Synchrotron site | APS |
Beamline | 22-BM |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2019-07-18 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 1.0 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 53.964, 81.769, 58.555 |
Unit cell angles | 90.00, 111.04, 90.00 |
Refinement procedure
Resolution | 54.650 - 2.010 |
R-factor | 0.1956 |
Rwork | 0.193 |
R-free | 0.24790 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | pdbid 2qzo |
RMSD bond length | 0.007 |
RMSD bond angle | 1.362 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0253) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 54.652 | 2.231 |
High resolution limit [Å] | 2.008 | 2.008 |
Rmerge | 0.099 | |
Number of reflections | 22425 | 1121 |
<I/σ(I)> | 13.8 | |
Completeness [%] | 92.5 | |
Redundancy | 7.6 | |
CC(1/2) | 0.999 | 0.544 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 298 | 20-25% PEG 3350, 200 mM MgCl2, 200 mM NaCl, 0.1 M Hepes pH 7 |